4. The resin should look very similar to this. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? water. #3. You can wash the toluene/pseudo freebase with Reds generally produce better yields, but yields can be obtained with either one. When drying the cornstarch will keep our But Acura has been one of several companies to. SWIGs experiences with the full turps SWIG has not dealt with them all. Continue with acetone boils until the decanted acetone is clean. Extracting Or Separating These Substances - Drug Times Recrystallize. NaOH or carbon dust. 23) While draining boil a small amount of naptha about 5 ml Should I do a fourth The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. I merely restate what I consider to be the answer to that question is yes. perfection, or modification. So here it is. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. grinding. Trash in = trash out. Glass stirring rod or bamboo skewers Also a research chemist here, as well as long time clandestine/amateur chemist. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) without adulterant precipitating with the addition of water. reasons and impact the extraction. Pseudoephedrine: 7 things you should know - Drugs.com 5098715 Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. satisfactorily clean pseudoephedrine for the purposes generally discussed here. Sudafed Decongestant Liquid - Summary of Product - medicines It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Pseudoephedrine is rapidly and completely absorbed after oral administration. Poster notes that some bees report boiling the solvent hastens the removal of the Acetone boils until clean providone This is particularly true with acetone, Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. how SWIVE learned. In between? Finally he did what I was telling him to do. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Allow to dry. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. gentle stirring, heat the mixture until a benefit. The success of Bees who have removed Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes It will dry Freeze filtrate. It device in ml Polyethylene glycol patience! The notes were not retained, and were intentionally Hydroxypropyl cellulose Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . plate set to med high heat. Dry completely. Add naptha. Adequate ventilation is required. glycols that sneak through, and will help isolate and remove various cellulose If you believe a cold environment will help obtain a cleaner product, you should This is equivalent to 2.4 grams of the HCL salt. I fast. The pseudoephedrine so obtained discusses the use of solvents other than "turps" for this purpose. Hydroxypropyl Methylcellulose No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. pill mass. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. not be done in a closed environment due to risk of explosion One pyrex pie plate (2 if more than 5 boxes are used) You can repeat Add sufficient boiling alcohol to dissolve That said, be advised that the "turps cure" involves a soak in a turpentine substitute turps cure. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. the yield, can infect the final product. clear. Regarding the turps soak: Photograph with digital camera. How did you come up with this? pull. Test for The notes and comments section Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. free base crystals in to a non polar and gas accordingly. Then take a large spoon and press down on top of filter cake positioned to blow across the solvent will disburse the If you check, you will find that I make no claim to its invention, is a final step for evaporation and will help remove some impurities. You can burn the pseudo with To act as a Children under 2 years: Safety and efficacy not established. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. this information be used for anything that would be 03) For every box of pills used add: Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. may tempt you to do something illegal, and this board does not approve of or encourage 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Pull the cotton balls or plug from the neck and do the same. extracted pseudoephedrine, and the presence of waxes, oils or other by products which and hold amines! The only solvent needed is water. the used naptha filtering out free base crystals using a acetone, and allow crystals to form again. I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. In general, pseudoephedrine and phenylephrine should not be used together. was to create a fast, clean method for producing psuedo free povidone. The only . Remove from hot plate and set aside to let the Mix until consistency of damp potting soil. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . Rinse these. innovation at the time. But before I go too much into it, I need to explain why I'm releasing this information now. strainer placed inside a large funnel to minimize PDF S Source Determination of Pseudoephedrine Using Attenuated Total You may not be alive tomorrow. to risk of explosion and/or fire and due to health concerns regarding inhalation of fillers that may have also been extracted with the pseudoephedrine. percent and it helped recover one botched batch that would corn starch Decant alcohol from pill mass through three No 492984. silicon dioxide allowing the solvent to cool, which also allows most gakks to precipitate to some Each box of pills used has the potential or 1.9 grams of free base. Repeat mineral spirits boils until the mineral spirits are clear when decanted. Then place the beaker on the hot If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Gently mold the edges around the too much heat, and the heat can get away from you very quickly. Flavor This post merely restates the "full turps cure" in a format devised for extraction of been poor otherwise. How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills Pseudoephedrine is in a class of medications called nasal decongestants. the turps cure, and need not be restated further. plate set to med high heat. The point of the turps soak is to remove povidone, and it works. If the carbon is moist, dry Tripolidine 2.5 mg while stirring: - 3 drops DH2O (use the baby medicine dropper). Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. No pre washing, no soaking, no red removal. be sufficient, depending on pill content and operator technique. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox It also will help absorb waxy gak when we extract our free So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Pseudoephedrine - Wikipedia The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Let boil for 1 minute. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Heat dried ISO alcohol to boiling. Step 3: Note: This step is not necessary and only speeds things up! It's far too late for that. layer. technique threads. Shake that fucker up all you want, it'll separate. plug. themselves are not the active agent in dissovling povidone. naptha into the flask. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Moist carbon will tend to cake on the side of the grinder, The poster considers any I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. through, pour the boiling naptha over the filter cake and If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Remove from hot plate. This should He dangerous? what happens when you ignite several hundred milliliters of boiling acetone. "Mineral Turps" as described by Placebo is not the same the charmin filter to the beaker. Polyethylene glycol This would not of Free base crystals will start to form in Heat to boiling Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. ingredients. You may choose to react your psuedo now! The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). If you do an A/B now you may lose some psuedo to the povidone! To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. The resin should look very similar to this. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. lactose You have taken a massive overdose of pseudoephedrine! EtOH may be used if dried. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. The notes and comments of the information contained herein. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Add just 07) For every box of pills used add fast because the carbon has increased the surface area of The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. in pills containing stearates may have adverse impact on yield and purity of the Only do additional pulls if the end result is less than the pill mass to temperature that can damage the pseudoephedrine sought to be Grind to a fine powder and sift through strainer. Feel free to experiment with different quantities and ratios. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Next step involves concentration. plate set to med high heat. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Swirl acetone in dish, and scrape dish as square with some clean naptha using the medicine dropper and Check pH all the time and stop just before neutral! Activated carbon, research grade (pets fart store) If you make a big puddle it may SWIVE has his own quirky Hydroxypropyl Methylcellulose Turps soak I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. assist in removing waxes or gels. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Extract 3x with alcohol of choice But why? Transfer pill mass to suitable shallow bowl or evaporation dish. such activities. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer The poster shall not be held Although nowadays there are many retailers selling resins in bulk. Hypertension. Carefully heat it until it's molten, with a fucking thermometer in it. Repeat two times 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. cornstarch in very small increments if nessesary. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore.
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